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GCMS analytical results for sample AE03825, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03825 analyzed on March 29, 2002.

NYC-WTC_000038032–000038041

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File C:\HPCHEM\l\DATA\MAR2202\3825.D Vial: 6 Acq On 22 Mar 2002 11:03 pm Operator: Sample gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Smoothing OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs 0.2 Max Peaks: 100 Stop Thrs 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.259 781 786 801 rVB 869284 2035455 67.50% 13.631% 2 15.904 1177 1183 1200 rBV 1340107 2721393 90.25% 18.224% 3 21.210 1755 1761 1774 rBV 1484223 3015282 100.00% 20.192% 4 25.653 2239 2245 2256 rBV2 1403346 .2 96692 0 98.40% 19.868% 5 30.730 2793 2798 2805 rVB 190250 368491 12.22% 2.468%

6 33.722 3114 3124 3138 rBV 909165 2134201 70.78% 14.292% 7 33.934 3142 3147 3155 rVB 38257 84901 2.82% 0.569% 8 37.395 3517 3524 3532 rBV2 10176 31734 1.05% 0.213% 9 37.973 3578 3587 3604 rBV 504737 1538040 51.01% 10.300% 10 38.854 3676 3683 3693 rBV4 10230 36441 1.21% 0.244%

Sum of corrected areas: 14932858

3825.D GCMS0308.M Tue Mar 26 14:54:17 2002

NYC-WTC_000038037

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NYC-WTC_000038037Source: NYC Law Department, mirrored locally

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