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GCMS analytical results for sample AE03823, March 29, 2002

Machine-extracted title · confidence 100%

Laboratory report listing detection results for volatile organic compounds in sample AE03823 analyzed on March 29, 2002.

NYC-WTC_000038013–000038021

Folder label: “GCMS X 2/20/02 A 3/22/02

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Scanned page image, NYC-WTC_000038018
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data. File : C:\HPCHEM\l\DATA\MAR2202\3823.D Vial: 14 Acq On : 23 Mar 2002 6 : 54 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.260 781 786 802 rVB 955366 2198710 67.00%• 13.825% 2 15.905 1177 1183 1200 rBV 1397201 2956229 90.08% 18.587% 3 21.211 1754 1761 1774 rBV 1611108 3281702 100.00% 20.634% 4 25.655 2238 2245 2256 rBV2 1503055 3171365 96.64% 19.940% 5 30.731 2793 2798 2808 rBV 222888 424256 12.93% 2.668%

6 33.715 3116 3123 3138 rBV2 1004341 2240724 68.28% 14.089% 7 33.926 3142 3146 3155 rVB 40015 85581 2.61% 0.538% 8 37.965 3577 3586 3604 rBV2 501785 1510715 46.03% 9.499% 9 38.856 3675 3683 3695 rBV3 8754 35140 1.07% 0.221%

Sum of corrected areas: 15904422

3823 .D GCMS0308.M Tue Mar 26 14:52:40 2002

NYC-WTC_000038018

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NYC-WTC_000038018Source: NYC Law Department, mirrored locally

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