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GCMS method 508 sample preparation log, March 22, 2002

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Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.

NYC-WTC_000037992–000037995

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document

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Jser: Galos, Marie Westchester Dept. of Labs & Research Date: 03/26/2002 Time: 16:06:40

Sample: AE03823 Analysis: SC1GCMS CALI GCMS Jnits: ug Started: 3/26/02 16:03 Ended: 3/26/02 16:03 Analyst: MG age: 1 Component Name 1 l n-Nitrosodimethylamine a; Viol 37.79 Result Qualifier JMDLE 2.0 -2 - . bis(2-Chloroethyl)ether — ----- ----- —------- —-— 37.24 2.0 3 ■ 1,3-Dichlorobenzene 38.73 2.0 4 ] 1,4-Dichlorobenzene 38.80 2.0 5 ■ 1.2-Dichlorobenzene 38.70 2.0 ?2' oxybis(1-Chloropropane) 35.86 2.0.... 7 ii-Nitrosodi-n-propylamine 38.07 2.0........ 8 Hi xachloroethane 38.55 2.0 9 Nitrobenzene 37.13 _ 2.0 2.0 10 Isophorone 37.12 d bis(2-Chloroethoxy)methane 37.40 2.0 Og 1,2,4-Trichlorobenzene 39.54 2.0 a Naphthalene 38.88 2.0 Hexachlorobutadiene 40.56 2.0 15 ji-Chioronaphthaiene 38.09 2.0 16 j Dimethylphthalate 38.41 2.0 6-Dinitrotoluene 38.59 . ... _. 2.0 18 Acenaphthylene 38.01 . 2.0........ 19 -i. enaphthene 37.98 2.0..... 202,4-Dinitrotoluene 37.80 _ _____ 2.0 21 Diethylphthalate 37.47 _________ 2.0 22 4-Chlorophenylphenylether 39.24 2.0 23 Fluorene 38.11 2.0 24 Azobenzene/1,2-Diphenylhydraz 34.09 2.0 25 |n-Nitrosodiphenylamine 35.77 2.0 264-Bromophenylphenylether 38.00 2.0 27 Hexachlorobenzene 37.38 2.0 Phenanthrene 36.79 2.0 2 9 Anthracene 36.67 ........ .... 2.0 30 Di-n butylphthalate 36.19 ............. 2.0 2.0 Fluoranthene 37.01 32 Pyrene 41.65 2.0 Butylbenzylphthalate 39.11 37.26 2.0 “Be Benzo(a)anthracene 2.0 bis(2-Ethylhexyl)phthalate 36.37 2.0 36 Chrysene 36.69 2.0 371 Di-n-octylphthalate Benzo(b)fluoranthene 41.18 39.80 2.0

384 39 .. Benzo(k)fluoranthene 40.43 2.0 _' 2.0 Benzo(a)pyrene 37.40 2.0 40 if Indeno(1 ,2,3-cd)pyrene 30.98 • ____ 2.0 42 Dibenz(a,h)anthracene 31.24 2.0 ' 43 Benzo(g,h,i)perylene 30.33 2.0

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