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GCMS quantitative results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.

NYC-WTC_000037870–000037883

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3799.D Vial: 9 Acq On : 19 Mar 2002 6:13 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclotetrasiloxane, octamet... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

8.91 0.82 ug/L 330537 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- ... 296 C8H24O4Si4 000556-67-2 91 2 Cyclotetrasiloxane, octamethyl- ... 296 C8H24O4Si4 000556-67-2 83 3 Cyclotetrasiloxane, octamethyl- ... 296 C8H24O4Si4 000556-67-2 78 4 7H-Dibenzo[b,g]carbazole, 7-methyl- 281 C21H15N 003557-9-1 59 Abundance Scan 643 (8.908 min): 3799.D (-) m/z 281.00 100.00% 2(11

5000

II—uufuuT 193 249265 8.60 8.80 9.00 9.20 , 57 73 103 133 0 TTTIAWTTTT Tpa 177 L m/z 282.10 28.73% "•i” m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #244216: Cyclotetrasiloxane, octamethyl- (CAS) $$ 1,1,3,3,... 261

5000 - - — —+ —P 8.60 8.80 9.00 9.20 m/z 283.10 16.13%

m/z—> Abundance 28 45 70 7 103 0 TTpUTTTTTT 133 I ........ g.l.. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #244217: Cyclotetrasiloxane, octamethyl- (CAS)$$ 1,1,3,3,... 281

T T T T ’I 8.60 8.80 9.00 9.20 5000 m/z 193.00 8.84%

133 45 73 eg 110 149165 191207 0 TBnI—uttumt—TpoerTIU—dpur TITT’TETTIIT—EET’TTTT _.. 249265.297 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #244218: Cyclotetrasiloxane, octamethyl- (CAS) $$ 1,1,3,3,... 281 ■ ■ i ■ ■ ■11 ■ i • • ■ ■ i • • ■ • i 8.60 8.80 9.00 9.20 m/z 191.00 8.54%

5000

73 193 45 | 133 177 1 । 221 249265 0 TTmOpunag" TTTTT . । >>*> । > 111।. 11 >I,11 j 11, —.297 T 1’ i •1 • • i •' ■ • i m/z- -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 8.60 8.80 9.00 9.20

3799.D 5080302.M Thu Mar 21 11:39:26 2002 Page 3 NYC-WTC_000037877

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