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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \MSDCHEM\ 1\DATA\ 030402\2339.D Vial: 11 Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclotetrasiloxane, octamet... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

8.94 0.56 ug/L 191130 1,4-Dichlorobenzene-d4 9.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclotetrasiloxane, octamethyl- 296 C8H24 i4 000556-67-2 72 2 Cyclotetrasiloxane, octamethyl- ... 296 C8H2404 14 000556-67-2 64 3 7H-Dibenzo[b,g]carbazole, 7-methyl- 281 C21H15N 003557-49-1 59 4 Cyclotetrasiloxane, octamethyl- ... 296 C8H2404Si4. 000556-67-2 56 Abundance Scan 646 (8.935 min): 2339.D (-) m/z 281.00 100.00% 2(11

. 5000

....... I E444 118 . . Q T T 8.60 8.80 9.00 9.20

m/z-> ---k 0 A 73 ,4133 193 ;20 40 60 80 100 120 140 160 180 200 220 240 260 280 249265 m/z 282.10 24.95%

Abundance #244220: Cyclotetrasiloxane, octamethyl- 281

5000' I , r‘’t I ‘ ‘ ' I T 8.60 8.80 9.00 9.20 m/z 283.00 20.10% 73 265 45 | 133 177 123208 235 [ 0 ।.... । .•... ।,.;. । . ।.... ।.... । i...]... ."i.. r. । .i ।.... ।.... । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #244221: Cyclotetrasiloxane, octamethyl- (CAS)$$ 1,1.3,3,... 201 .................. I*' • * I ‘ J ‘ ‘ • I ‘ ‘ ‘ I 8.60 8.80 9.00 9.20 5000 m/z 265.00 9.03%

83 133 192207 249265 MAaBapahaa m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #227246: 7H-Dibenzo[b,g]carbazole, 7-methyl- 281 T 8.60 8.80 9.00 9.20 m/z 193.00 8.33%

5000

266 133

m/z—> 0 39 8387.. 11344,418318721323%. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 I “ “ I 8.60 8.80 9.00 9.20 T

2339.D 5080302.M Mon Mar 18 08:32:38 2002 Page 3

NYC-WTC_000010617

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NYC-WTC_000010617Source: NYC Law Department, mirrored locally

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