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GCMS analysis results for sample AE03617, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.

NYC-WTC_000037800–000037818

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037802
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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02MAR08\03617.D Vial: 7 Acq On : 8 Mar 2002 8:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 15 10:05:22 2002 Quant Results File: HP022102.RES

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP022102 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 2039629 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 8704676 20.00 ug/L 0.00 17) Acenaphthene-diO 18.33 164 4337042 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 7085162 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 5511021 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 3661368 20.00 ug/L -0.04 System Monitoring Compounds 37) 2,4-DDD 27.72 235 464877 4.92 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.40% Target Compounds Qvalue 20) Dimethylphthalate 18.33 163 689707 2.62 ug/L # 58 21) 2,6-Dinitrotoluene 18.33 165 556180 9.15 ug/L # 27 42) Bis (2-ethylhexyl) phthalat(31-09149 60531 0.26 ug/L 94

(#) = qualifier out of range (m) = manual integration 03517.D HP022102.M Fri Mar 15 10:05:23 2002 Page 1

NYC-WTC_000037802

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NYC-WTC_000037802Source: NYC Law Department, mirrored locally

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