GCMS blank results for sample AE03614, March 28, 2002

NYC 9/11 Public Portal Document . Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.12 ug/L 57534 1,4-Di chiorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 90 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 4 Thietane (CAS) $$ Thiacyclobutan... 74 C3H6S 000287-27-4 43 Abundance Scan 10 (3.487 min): 03514.D (-) m/z 74.00 100.00% 74

5000 47 82 P’ 3.50 3.60 3.70 3.80 3.90 0! T’2tt) -1 m/z 81.90 60.29% ’.It I ■ r ■ * »— । i ■ । i i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74

5000 47 82 AL t . 1‘‘ ‘1‘‘1171111 r-r 3.50 3.60 3.70 3.80 3.90 35 m/z 76.00 37.44%

miz-> 0! —......... .. .... IL... 10 20 30 40 50 60 _________ L ' i ■ ‘ 70 ■ i ' 80 90 - 109 ■ 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- 74 82 ’rI i ■ ■ ■ ■ i ■ ■ ‘ । 3.50 3.60 3.70 3.80 3.90 5000 m/z 83.90 36.49% __—_ 47 35 , 12 , - _________ L I 108 0! 1 I ' ‘ ‘ I ' 111 1 ' I ‘ ' I " ' 1 I ' " miz—> 10 20 30 40 50 60 70 90 80 100 110 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- 74 ' 13.50 3.60 3.70 3.80 3.90 m/z 47.00 29.48% 47 82 5000

miz—> 0 11+,11/1/B.11/111.8 10 20 30 38

। ■ ■ 40 50 ................... I 60 70 11t 80 । 1ITTTT 90 95 102108 100 110 AA... A 3.50 3.60 3.70 3.80 3.90

03514.D HP022102.M Fri Mar 15 10:09:22 2002 Page 3

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