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GCMS analysis results for sample AD30016, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30016 conducted on January 28, 2002.

NYC-WTC_000037244–000037254

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\1\DATA\JAN1502\30016.D Vial: 25 Acq On : 15 Jan 2002 3:49 pm Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.443 257 261 294 rBV 435940 1201649 11.78% 2.353% 2 10.978 640 646 657 rVB 46671 121430 1.19% 0.238% 3 11.501 697 703 721 rBV 3130924 7931959 77.74% 15.534% 4 14.145 985 991 997 rBV 63947 127420 1.25% 0.250% 5 15.100 1088 1095 1112 rBV 4447841 9746473 95.52% 19.088%

6 20.360 1660 1668 1691 rBV 4647547 10203280 100.00% 19.983% 7 24.776 2141 2149 2161 rBV2 4164199 9228506 90.45% 18.073% 8 29.852 2696 2702 2712 rBV 445088 872040 8.55% 1.708% 9 32.808 3017 3024 3049 rBV 2757364 6497280 63.68% 12.725% 10 36.875 3458 3467 3495 rBV 1851944 5131027 50.29% 10.049%

Sum of corrected areas: 51061064

30016.D GCMS1126.M Fri Jan 18 14:50:03 2002

NYC-WTC_000037249

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NYC-WTC_000037249Source: NYC Law Department, mirrored locally

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