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GCMS analysis results for sample AD31466, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31466 conducted on February 11, 2002.

NYC-WTC_000018405–000018415

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018410
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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\1\DATA\JAN1602\31466.D Vial: 25 Acq On : 17 Jan 2002 12:04 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.444 258 261 297 rVB 334678 1076167 16.81% 3.195% 2 11.502 698 703 724 rBV 1844754 4921907 76.90% 14.613% 3 15.091 1089 1094 1112 rBV 3015871 6239148 97.48% 18.524% 4 20.361 1661 1668 1687 rBV 3054007 6400192 100.00% 19.002% 5 24.776 2142 2149 2161 rBV2 2663305 5994342 93.66% 17.797%

6 26.025 2280 2285 2292 rVB2 80557 148461 2.32% 0.441% 7 29.853 2696 2702 2709 rBV 379281 772240 12.07% 2.293% 8 31.496 2876 2881 2889 rVB 59342 114521 1.79% 0.340% 9 32.800 3017 3023 3042 rBV2 1925257 4524170 70.69% 13.432% 10 36.867 3459 3466 3492 rBV 1295948 3490208 54.53% 10.362%

Sum of corrected areas: 33681356

31466.D GCMS0103.M Thu Feb 07 12:42:14 2002

NYC-WTC_0000 18410

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NYC-WTC_000018410Source: NYC Law Department, mirrored locally

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