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GCMS analysis results for sample AD29781, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD29781 conducted on January 9, 2002.

NYC-WTC_000037197–000037206

Folder label: “GCMS X 12/10/01 A 12/15/01

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Scanned page image, NYC-WTC_000037202
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29781.D Vial: 48 Acq On : 16 Dec 2001 12:35 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Smoothing OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs 0.2 Max Peaks: 100 Stop Thrs 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak %. of # min scan scan scan TY height area % max. total

1 7.600 274 278 290 rBV 349992 974457 14.09% 2.832% 2 7.728 2 90 292 309 rVB 51165 211281 3.05% 0.614% 3 11.667 716 721 745 rBV 1750700 4874688 70.48% 14.168% 4 15.274 1109 1114 1133 rBV 2807968 6313331 91.28% 18.349% 5 20.553 1683 1689 1713 rBV 3091259 6916405 100.00% 20.102%

6 24.969 2164 2170 2183 rBV2 2645595 6303645 91.14% 18.321% 7 30.055 2718 2724 2732 rBV 358679 754244 10.91% 2.192% 8 33.011 3039 3046 3064 rBV 1925576 4656767 67.33% 13.534% 9 37.096 3484 3491 3514 rBV2 1135090 3402218 49.19% 9.888%

Sum of corrected areas: 34407036

29781.D GCMS1126.M Fri Dec 28 14:51:48 2001

NYC-WTC_000037202

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NYC-WTC_000037202Source: NYC Law Department, mirrored locally

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