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GCMS analysis results for sample AD29732, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29732 conducted on January 7, 2002.

NYC-WTC_000037018–000037028

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29732.D Vial : 9 Acq On : 15 Dec 2001 10:20 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.77 ug/1 214381 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual.

1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H1603 020324-32-7 90 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propanol, 1- (2-methoxypropoxy) - 148 C7H16O3 013429-07-7 47 4 2-Pentanol, 2-methyl- 102 C6H140 000590-36-3 42 ’Abundance Scan 686 (11.345 min): 29732.D (-) m/z 59.05 100.00% 59

5000- 45 103 73 V

miz—> 20 -ll— 30 40 50 — 'r — 60 70 80 85..... ।.............. 90 100 110 120 130 140 11.00 m/z 11.20 45.05 11.40 11.60 45.31% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000- V 45 103 11.00 11.20 11.40 11.60 73 31 m/ z 103.05 33.49% i ............................................. ,.........................130........... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3-oxybis- 59 I*1 11.00 11.20 11. : 11.60 5000- 31 45 m/z 73.00 27.06%

VA 103 I . i l : ........... ■................... .......................1.............................. 134 , ‘I’’ TT 1Er‘nLB miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 'Abundance #9233: 2-Propanol, 1 -(2-methoxypropoxy) T1 59 11.00 11.20 11.40 11.60 m/ z 41.00 0, 23.52%

m/z-> 5000

31 ,1— T ■ । ' ■ ' ■ । ■ • i ' ■ ■ ' i‘ ■ 20 30 40 45 —A......... Pl4............. ....... 50 60 70 80 90 100 110 120 130 140 11.00 11.20 UUA 11.40 11.60

29732.D GCMS1126.M Fri Dec 28 13:10:18 2001 Page 2

NYC-WTC_000037026

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NYC-WTC_000037026Source: NYC Law Department, mirrored locally

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