GCMS analysis results for sample AD29665, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29665.D Vial: 10 Acq On : 15 Dec 2001 11:19 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 4.65 ug/.l 1166500 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 entative ID MW MolForm CAS# Qual

1 N- Ethyl formamide 73 C3H7NO 000627-45-2 9 2 1, 3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3 -Dixolane , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 277 (7.590 min): 29665.D (-) m/z 73.00 100.00% 73

5000- 43

3? |, | 50 55 60 67. । 87 103 7.20 7.40 7.60 7.8017 8.00 i ■ ■ ■ • i ■ > ■ • i ■ 1 r1 ' 1 1 1 1 TnT . • . ■ I m/z 43.05 28.54% m/z-> 10 20 30 40 50 60 70 80 90 100 110 (Abundance #292: N-Ethylformamide 30 73

5000- —1 —IT ' 1 ‘ ’ TT 58 7.20 7.40 7.60 7.80 8.00 44 m/z 45.05 10.49% 15 m/z-> l'1' ' I 10 20 30 .....401—— 50 60 70 80 90 100 110 Abundance #62902: 1.3-Dioxolane, 2-methyl- 73 - 7.20 7.40 .60 7.80 8.00 5000 43 m/z 41.00 10.48%

miz-> Abundance i ' ■ ■ ■ i 10 20 27. • 60 58 I I • k • ■ I > » • < l • • • • l • ' ■ ■ l • ■ • • l 30 40 50 70 #1793: Pentane, 3-methoxy- 80

73 87 L 90 100 110

7.20 m/ z T i TTTmR—T 7.40 7.60 71.0.0 L 7.80 8.00 6.55% 5000 - 45

27 33 39 i ■ ' 1 1 i ■ ■ ' ■ i ' ' ' ' i 1 ' ' TI 55 —IP 1— i ' ' 1 • 1 1 1 1 ' 1 1 ------- I I -I T I I I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29665.D GCMS1126.M Fri Dec 28 13:09:07 2001 Page 1

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