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GCMS analysis results for sample AD29665, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29665 conducted on January 7, 2002.

NYC-WTC_000037007–000037017

Folder label: “GCMS X 12/10/01 A 12/15/01

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Scanned page image, NYC-WTC_000037015
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29665.D Vial: 10 Acq On : 15 Dec 2001 11:19 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************* *.* ****************************** Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 1.08 ug/1 270625 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1/(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 2-Butanol, 3,3 1 -oxybis- 162 C8H18O3 054305-61-2 64 3 2 -Propanol, 1,1‘ -oxybis- 134 C6H14O3 000110-98-5 56 4 2-Propano/, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 Abundance Scan 685 (11.336 min): 29665.D (-) m/z . 59.05 100. 00% 59

mlz-> 5000

20 ■ i ■ ' ■ ' । ' 30 , 31 40 45

—5051 460PH70 — 73

80 85 ■ i ■ ' 1 ■ i ' 90 103

1 1 1 T—-r . ) 100 110 I .... 1 . I I 1 1 . 120 130 140 • ’ i ' 11.00 m/z I ■ • • ■ l • • ■ ' I 11.20 45.05 N11.40 11.60 52.10% Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy)

5000 T T 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.00 33.53% ........... !.......... 130.... —....... —........ 1T ....।। m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance 412859: 2-Butanol, 3,3°-oxybis- 59 11.00 1120 11.40 11:60 5000 31 m/z 73.00 28.58% 45 103

mlz-> Abundance 20 .1 ' I ' ■ ' ' I ' ' ' ' I ' 30 40 50 60

59 ..................................................................................... 134 , 70 80 90 100 #6087: 2-Propanol, 1,1'-oxybis- 110 120 130 140 I 1 ' T~' 1 11.00 11.20 m/ z 41.05 C3 V/ T 11.40 ■ i ■ ■ ■ ■ i 11.60 25.93%

NN 31 5000 45

103 - 72 89 TPH------------------- TrrreTTrr ' ' i ' ' ' ' I ' ' ' ' I m/z--> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29665.D GCMS1126.M Fri Dec 28 13:09:11 2001 Page 2

NYC-WTC_000037015

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NYC-WTC_000037015Source: NYC Law Department, mirrored locally

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