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GCMS analysis results for sample AD29665, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29665 conducted on January 7, 2002.

NYC-WTC_000037007–000037017

Folder label: “GCMS X 12/10/01 A 12/15/01

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Scanned page image, NYC-WTC_000037012
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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\l\DATA\DEC1401\29665.D Vial: 10 Acq On : 15 Dec 2001 11:19 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.590 273 277 310 rBV 394641 1166502 17.90% 3.421% 2 11.336 681 685 691 rBV 113112 270625 4.15% 0.794% 3 11.419 691 694 714 rVB 128818 378797 5.81% 1.111% 4 11.676 714 722 741 rBV2 1825860 5013717 76.93% 14.703% 5 15.274 1108 1114 1133 rBV 2682799 5987121 91.87% 17.557%

6 20.553 1683 1689 1706 rBV 3007778 6517005 100.00% 19.111% 7 24.969 2164 2170 2183 rBV2 2624078 6119455 93.90% 17.946% 8 30.055 2718 2724 2731 rBV 405420 840004 12.89% 2.463% 9 33,. 011 3039 3046 3064 rBV 1885050 4514766 69.28% 13.240% 10 37.096 3483 3491 3507 rBV2 1137397 3292088 50.52% 9.654%

Sum of corrected areas: 34100080

29665.D GCMS1126.M Fri Dec 28 13:08:52 2001

NYC-WTC_000037012

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NYC-WTC_000037012Source: NYC Law Department, mirrored locally

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