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GCMS analysis results for sample AD29787, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29787 conducted on January 7, 2002.

NYC-WTC_000036995–000037006

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC14O1\29787. D Vial: 12 Acq On 15 Dec 2001 1:16 pm Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.60 ug/1 144205 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 28 2 Glycine, N-acetyl- 117 C4H7NO3 000543-24-8 4 3 Cyclopentanol, 2-methyl-, acetate, 142 C8H14O2 040991-94-4 4 4 2-Propanone, 1,1-dichloro-________ 126 C3H4C120______ 000513-88-2 4 'Abundance Scan 294 (7.741 min): 29787.D (-) m/z 4 .00 100.00% 43

5000-

P —7.40 7.60 7.80 8.00____ • ■ । ■ ' ■ ' ।' ■ ■ i ■ HT+ 1 ' 49 37 1 i ■ 55 ■ 61i 71 82,88. । . . 97,103 TCInnT 1 117 127 . > । .i . . । TT । TT । । । m/ z 126.90 7.93% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 4|3

5000 7.40 7.60 7.80 8.00 15 m/z 124.95 7.82% — I , 35 11 ' 1 1 49 85 97 117 125 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3394: Glycine, N-acetyl- 30 43 7.40 7.60 7.80 8.00 5000- m/z 96.85 6.58% 72 15 t 56 99 I i 117 TT —— I 1 'I 1 ' 1 1 I ' .......... | 1 | I I | I I I ‘1—tr I | I I Cl | I I I I | | I m/z-> 10 20 30 40 50 60_70 80 90__ 100 110 120 130 'Abundance #7952: Cyclopentanol, 2-methyl-, acetate, trans- • • l • • • ‘ | । । । । i . । । 43 7.40 7.60 7.80 8.00 m/z 81.85 5.42% 5000 82 67 55 , 100 .. ..... ..... I,i,.. 1 __ L ''I'' * '1 1 ' * ' I 1 11 1 I ' 1 1 1 I 1 1,1 1 1 111 1 1 1 1 ' i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00

29787.D GCMS1126.M Fri Dec 28 13:22:45 2001 Page 2

NYC-WTC_000037003

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