GCMS analysis results for sample AD29564, Jan 2002

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GCMS analysis report for sample AD29564 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036915–000036926

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1301\29564.D Vial: 25 Acq On : 14 Dec 2001 8:20 am . \WA/ Operator: 209 GALOS Sample : gems scan 12/7 A 1 6—rI) Inst : GC/MS 209 Multiplr: 1.00 MS Integration Params: RTEINT.P • Quant Time: Dec 27 15:08 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1150310 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 4400842 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 2239676 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3154521 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 2022301 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1396086 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.05 235 136091 2.98/g/mL . 02 Spiked Amount 5.000 Recovery = / 59.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.14 74 561 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.03 77 174 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1483 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate . 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.57 153 185 N.D. 24) 2,4-Dinitrotoluene 21.17 165 500 N.D. 25) Diethylphthalate 22.10 149 1108 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29564.D GCMS1126.M Thu Dec 27 15:18:07 2001 Page 1

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GCMS analysis results for sample AD29669, Jan 2002 · Box DEP Box 22

NYC-WTC_000036902

GCMS analysis report for sample AD29669 listing unknown compounds and surrogate recovery data from January 28, 2002.

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