NYC-WTC_000036888
GCMS analysis report for sample AD29668 listing unknown compounds and surrogate recovery data from January 28, 2002.
Same agency, volume and box · similarity 0.999
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GCMS analysis results for sample AD29669, Jan 2002
Machine-extracted title · confidence 100%GCMS analysis report for sample AD29669 listing unknown compounds and surrogate recovery data from January 28, 2002.
NYC-WTC_000036902–000036914Folder label: “GCMS X 12/7/01 A 1/2/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
"Data File : C:\HPCHEM\1\DATA\DEC1301\29669.D Vial: 23 Acq On : 14 Dec 2001 6:22 am Operator: 209 GALOS Sample : gems scan 12/7 OJAY Inst : GC/MS 209 Mise Multiplr: yydtant Results File: 1.00 GCMS112 6.RES MS Integration Params: RTEINT.P Quant Time: Dec 27 15:07 2001
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Thu Dec 13 14:40:46 2001 Response via Initial Calibration DataAcq Meth GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1329242 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 5089392 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2509519 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 3629398 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 2283567 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1596583 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 154798 2.95 ug/mL -0.02 Spiked Amount 5.000 Recovery = 59.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.19 74 846 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.30 117 419 N.D. 11) Nitrobenzene 13.30 77 175 N.D. 12) Isophorone 13.86 82 111 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 3354 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.23 165 486 N.D. 25) Diethylphthalate 22.08 149 1320 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 23.07 77 556 N.D.
(#) = qualifier out of range (m) = manual integration 29669.D GCMS1126.M Thu Dec 27 15:23:15 2001 Page 1
NYC-WTC_000036907
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