GCMS analysis results for sample AD29669, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\29669.D Vial: 61 Acq On 3 Jan 2002 1:04 am Operator: 209 GALOS Sample gems scan 12/7 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 16 9:12 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update Response via DataAcq Meth : : : Fri Dec 28 15:11:00 2001 Initial Calibration GCMS1126 34a— Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1217126 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 4737393 20.00 ug/1 -0.02 17) Acenaphthene-dlO 20.56 164 2390704 20.00 ug/1 -0.02 29) Phenanthrene-dlO 24.99 188 3361693m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 2103176 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1166504 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 127665 3.45 ug/mL 0.00 Spiked Amount 5.000 Recovery = 69.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.35 74 178 N.D. 3) bis(2-Chloroethyl)ether 10.68 93 117 N.D. 4) 1,3-Dichlorobenzene 11.72 146 494 N.D. 5) 1,4-Dichlorobenzene 11.72 146 494 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 12.94 70 25049 0.52 ug/1 # 58 9) Hexachloroethane 13.33 117 366 N.D. 11) Nitrobenzene 13.33 77 291 N.D. 12) Isophorone 14.12 82 915 N.D. 13) bis(2-Chloroethoxy)methane 14.32 93 1877 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 4917 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.53 162 135 N.D. 20) Dimethylphthalate 20.01 163 816 N.D. 21) 2,6-Dinitrotoluene 20.28 165 3744 N.D. 22) Acenaphthylene 20.12 152 737 N.D. 23) Acenaphthene 20.64 153 901 N.D. 24) 2,4-Dinitrotoluene 21.28 165 1055 N.D. 25) Diethylphthalate 22.11 149 3323 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.23 166 1091 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29669.D GCMS1126.M Wed Jan 16 09:13:10 2002 Page 1

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