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GCMS analysis results for sample AD29668, Jan 2002

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GCMS analysis report for sample AD29668 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036888–000036901

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\29668.D Vial: 65 Acq On 3 Jan 2002 4:57 am Operator: 209 GALOS Sample Mise gems scan 12/7

MS Integration Params: RTEINT.P Quant Time: Jan 16 14:38 2002 goT Inst Multiplr:

Quant Results File: : GC/MS 209 1.00

GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1259281 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 5113822 20.00 ug/1 -0.02 17) Acenaphthene-dlO 20.56 164 2599785 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 3793534m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 24 0 2482333m 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1422950m 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 179540 4. ug/mL 0/.00 Spiked Amount 5.000 Recovery 86.00%/

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.31 77 201 N.D. 12) Isophorone 14.31 82 1360 N.D. 13) bis(2-Chloroethoxy)methane 14.31 93 887 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1692 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.28 163 6437 N.D. 21) 2,6-Dinitrotoluene 20.28 165 3181 N.D. 22) Acenaphthylene 20.29 152 1283 N.D. 23) Acenaphthene 20.58 153 113 N.D. 24) 2,4-Dinitrotoluene 21.36 165 368 N.D. 25) Diethylphthalate 22.11 149 3168 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29668.D GCMS1126.M Wed Jan 16 15:31:07 2002 Page 1

NYC-WTC_000036890

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NYC-WTC_000036890Source: NYC Law Department, mirrored locally

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