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GCMS analysis results for sample AD29668, Jan 2002

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GCMS analysis report for sample AD29668 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036888–000036901

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC3101\29668.D Vial: 65 Acq On 3 Jan 2002 4:57 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 16 14:38 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. d 32) Hexachlorobenzene 0.00 284 0 N.D. d 33) Phenanthrene 0.00 178 0 N.D. d 34) Anthracene 0.00 178 0 N.D. d 35) Di-n-butylphthalate 0.00 149 0 N.D. d 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. d 41) Benzo(a)anthracene 0.00 228 0 N.D. 42) Bis(2-ethylhexyl)phthalate 0.00 149 0 N.D. d 43) Chrysene 0.00 228 0 N.D. 45) Di-n-Octylphthalate 35.04 149 1355 N.D. 46) Benzo(b)fluoranthene 35.57 252 645 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.11 252 6076 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29668.D GCMS1126.M Wed Jan 16 15:31:12 2002 Page 2

NYC-WTC_000036891

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NYC-WTC_000036891Source: NYC Law Department, mirrored locally

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