GCMS analysis results for sample AD29668, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU-l\209\DATA\DEC1301\29668.D Vial: 22 Acq On : 14 Dec 2001 5:24 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.08 ug/1 1041110 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual Silane, tetramethyl- 1 88 C4H12Si 000075-76-3 23 N-Ethyl formamide 2 73 C3H7NO 000627-45-2 9 1,3-Dioxola: 3 2-(3-bromo-5,5,5-tri 352 C10H16BrC1302 000000-00-0 9 3-Pentanol, 3-methyl- 4 102 C6H140 000077-74-7 9 Abundance Scan 278 (7.595 min): 29668.D (-) m/ z "100.00% 73

5000 - 43 | 7.20 7.40 7.60 7.80 8.00 i 37, |, | 50 55 60 67, 1 1........87...........103................ ' ' I ' • ' ' I ' ' ' ' I ' ' ' ' I 1 1 • ' I ''''l' ' ' T * m/z 43.00 27.85% m/z-> 10 20 30 40 50 60 70 80 90 100 116 120 'Abundance #62932: Silane, tetramethyl- i 73

5000 7.20 7.40 7.60 7.80 8.00 45 m/ z 44.95 10.52% 15 1 53 59 I .......... 88........................................ m/z->10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 7.20 7.40 7.60 7.80 8.00 5000- m/z 41.05 9.79% 44 58

5......I , nn rYi-r-T-T-pr-rTr-T-pr-T-rT-p-r-r I..................................... m/z-> 1G 20 30 40 50 60 70 80 90 100. 110 120 'Abundance #49423: 1,3-Dioxolane. 2-(3-bromo-5,5,5-trichloro-2,2-dimet ----- ■ i ■ ■ 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.54% 5000-

45

36 11 ' I ' 1 ' ' I ' ' ' ' I ' ' 1 ' I ' 55 BdOmrrd. 67. ..................................... 109 1,15 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 3.00

29668.D GCMS1126.M Tue Jan 08 10:58:48 2002 Page 1

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