GCMS analysis results for sample AD29564, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\2O9\DATA\DEC13O1\29564.D Vial: 25 Acq On : 14 Dec 2001 8:20 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method,: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 2.57 ug/1 835458 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 32 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 7 4 2-Propanol, 1 -amino- 75 C3H9NO 000078-96-6 5 Abundance Scan 278 (7.600 min): 29564.D (-) m/ z 73.00 100.00% 73

j 5000 43 7.20 7.40 4 7.60 7.80 8.00 38 | 50 55 61 67, , 1........ 87 .......... 103 i 1 1 ' ' i 1 ' ' ' i ' I 1 1 ■ ' i ' ■ ■' ■' I ' ' ' ■ I m/z 43.00 27.02% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 713

5000 7.20 7.40 7.60 7.80 8.00 45 m/z 41.05 11.12% i । 15 ■ ■ । ■ , .1 l • ■ • • । ■ . ■ ■ । I > ■ ■ । 53 ‘ 59 ‘। » । ' I.............. 88................................ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformarnide 30 73 -T — — । -= 7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 10.06% 44 58

— .! i . I । ' ■ 1 I ' ' * ' I ' 1 m/z--> ____ 10 20 30 40 50 60 70 80 90 100 110 ■Abundance #62903: 1,3-Dioxolane, 2-methyl- Tl • ■ ■ 1 | ■ ■ ■ ■ | • TTTr ■ | ■ 73 7.20 7.40 7.60 7.80 8.00 43 m/z 71.00 6.66% ! 5000 27 58 87 ■ • i ■ > • > t 1 1 ' 1 I — > • i ■ • ' । ' ' ' ■ i 1 1 1 1 i ■ ' ' ■ । ■ 1-1 ' i 1 1 1 1 i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29564.D GCMS1126.M Tue Jan 08 10:56:28 2002 Page 1

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