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GCMS analysis results for sample AD29671, Jan 2002

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GCMS analysis report for sample AD29671 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036860–000036873

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN0302\29671.D Vial: 13 Acq On 3 Jan 2002 10:17 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise . Multiplr: 1.00 MS Integration Params: GOOFY.P, Quant Time: Jan 15 15:58 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.88 178 769 N.D. 34) Anthracene 25.01 178 202 N.D. 35) Di-n-butylphthalate 26.82 149 89548 0.33 ug/1 # 98 36) Fluoranthene 28.49 202 427 N.D. 39) Pyrene 29.17 202 421 N.D. 40) Butylbenzylphthalate 31.33 149 1679 N.D. 41) Benzo(a)anthracene 32.84 228 8919 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 50524 0.29 ug/1 # 91 43) Chrysene 32.84 228 8919 N.D.. 45) Di-n-Octylphthalate 34.89 149 2860 N.D. 46) Benzo(b)fluoranthene 35.89 252 2104 N.D. 47) Benzo(k)fluoranthene 35.94 252 2560 N.D. 48) Benzo(a)pyrene 36.76 252 2134 N.D. 49) Indeno(1,2,3-cd)pyrene 40.50 276 197 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.58 276 568 N.D.

(#) = qualifier out of range (m) = manual integration 29671 .D GCMS1126,M Tue Jan 15 15:59:35 2002 Page 2

NYC-WTC_000036863

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NYC-WTC_000036863Source: NYC Law Department, mirrored locally

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