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← Document results/DEP Box 22/GCMS X 12/7/01 A 1/2/02
Document / 27 pages

GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036771
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Methanone, [1,4-dimethyl-7-(1- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

32.42 6.66 ug/1 13887800 Chrysene-dl2 33.05

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Methanone, [1,A-dimethyl-7-(1-methy 302 C22H220 039665-56-0 25 2 Phosphonic a d, phenyl-, bis(trime 302 C12H2303PSi2 042449-24-1 12 3 3 -Methoxyben oic acid, TMS 224 CllH16O3Si 000000-00-0 11 4 1-Hydroxy- ,7,8-trimethoxyxanthen-9 302 C16H1406 000000-00-0 10 Abundance Scan 2982 (32.424 min): 29522.D (-) m/z 287.10 100.00% 287

302 209 5000- 105 165 223 77 91 —I-------

m/z-> Abundance 0- 51 1 128 147 374 80 100 120 140 160 180 200 220Pmmapum 40 60 Hl“m." 14 239253 271’ I L&L 340 240 260 280 300 320 340 #43214: Methanone, [1,4-dimethyl-7-(1-methylethyl)-2-azulen 11 1 11 32.00 32.20 32.40 32.60 32.80 m/ z 3 02.20 59.95%

77 302 105 287

5000- Ti," 1 | 1 . ‘ | < . I I | ! ! 32.00 32.20 32.40 32.60 32.80 165 197 m/z 2 09.05 51.96% 1 I 216 244258273 • i ■ ■■■ i ■ ''I ■ T i] i'''' i'1' ■ i ‘' r ‘' i miz-> 4G 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43026: Phosphonic acid, phenyl-, bis(trimethylsily!) ester 287

32.00 32.20 32.40 32.60 32.80 .5000 m/z 105.05 41.61% 302 73 121135 195 211i _____ 271 ‘ I ''' [ • ■ ■' । 1 TTI 111 ’' I'1'11 i' ■ ■1 r ' ■' i''' ■ I '' ‘' I ‘' I ’ ‘ ‘' i' ‘ ‘' I ' ' i ■ ■' ■ i mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #28574: 3-Methoxybenzoic acid, TMS !t.T * » i • • • • । ' 1 209 32.00 32.20 32.40 32.60 32.80 m/z 165.10 32.45% 135 5000- 165 224

m/z-> 47 ' 1 I '' 1 ' i 40 60 + TTr 77 92 107

80 1 194 TITrt‘1."‘11"-TIT——IIT-TITTrT '' i''' ■ i' ■'' i'' '' I 100 120 140 160 180 200 220 240 260 280 300 320 340 It" ----- 32.00 32.20 32.40 32.60 32.80

29522.D GCMS1126.M Fri Jan 18 16:49:10 2002 Page 14

NYC-WTC_000036771

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NYC-WTC_000036771Source: NYC Law Department, mirrored locally

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