NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\29522.D Vial: 63
Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title 209 625/TCLP calibration table
Library C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 14 Methanone, [1,4-dimethyl-7-(1- Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
32.42 6.66 ug/1 13887800 Chrysene-dl2 33.05
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Methanone, [1,A-dimethyl-7-(1-methy 302 C22H220 039665-56-0 25
2 Phosphonic a d, phenyl-, bis(trime 302 C12H2303PSi2 042449-24-1 12
3 3 -Methoxyben oic acid, TMS 224 CllH16O3Si 000000-00-0 11
4 1-Hydroxy- ,7,8-trimethoxyxanthen-9 302 C16H1406 000000-00-0 10
Abundance Scan 2982 (32.424 min): 29522.D (-) m/z 287.10 100.00%
287
302
209
5000- 105
165 223
77 91 —I-------
m/z->
Abundance
0-
51 1 128 147
374 80 100 120 140 160 180 200 220Pmmapum
40 60
Hl“m." 14 239253 271’ I
L&L 340
240 260 280 300 320 340
#43214: Methanone, [1,4-dimethyl-7-(1-methylethyl)-2-azulen
11 1 11
32.00 32.20 32.40 32.60 32.80
m/ z 3 02.20 59.95%
77 302
105
287
5000- Ti,"
1 | 1 . ‘ | < . I I | ! !
32.00 32.20 32.40 32.60 32.80
165 197 m/z 2 09.05 51.96%
1 I 216 244258273
• i ■ ■■■ i ■ ''I ■ T i] i'''' i'1' ■ i ‘' r ‘' i
miz-> 4G 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #43026: Phosphonic acid, phenyl-, bis(trimethylsily!) ester
287
32.00 32.20 32.40 32.60 32.80
.5000 m/z 105.05 41.61%
302
73
121135 195 211i _____ 271 ‘ I
''' [ • ■ ■' । 1 TTI 111 ’' I'1'11 i' ■ ■1 r ' ■' i''' ■ I '' ‘' I ‘' I ’ ‘ ‘' i' ‘ ‘' I ' ' i ■ ■' ■ i
mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
'Abundance #28574: 3-Methoxybenzoic acid, TMS !t.T * » i • • • • । ' 1
209 32.00 32.20 32.40 32.60 32.80
m/z 165.10 32.45%
135
5000- 165
224
m/z->
47
' 1 I '' 1 ' i
40 60
+ TTr
77 92 107
80
1 194
TITrt‘1."‘11"-TIT——IIT-TITTrT
'' i''' ■ i' ■'' i'' '' I
100 120 140 160 180 200 220 240 260 280 300 320 340
It" -----
32.00 32.20 32.40 32.60 32.80
29522.D GCMS1126.M Fri Jan 18 16:49:10 2002 Page 14
NYC-WTC_000036771
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