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GCMS calibration data for sample AD29522, Jan 2002

Machine-extracted title · confidence 95%

Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.

NYC-WTC_000036695–000036702

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC3101\LBF.D Vial: 59 Acq On 2 Jan 2002 11:08 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.614 275 280 312 rBV 621804 2009585 11.61% 2.300% 2 11.672 717 722 751 rBV 5145547 13445849 77.67% 15.392% 3 15.280 1109 1115 1134 rBV 6509581 16290871 94.10% 18.649% 4 20.568 1683 1691 1717 rBV2 6898783 17312618 100.00% 19.818% 5 24.993 2165 2173 2219 rBV2 5-917470 17079091 98.65% 19.551%

6 30.069 2720 2726 2739 rBV 449280 1049936 6.06% 1.202% 7 33.034 3041 3049 3074 rBV2 4434539 12145952 70.16% 13.904% 8 37.129 3486 3495 3528 rBV 2405914 8023520 46.34% 9.185%

Sum'of corrected areas: 87357422

LBF.D GCMS1126.M Wed Jan 16 15:07:35 2002

NYC-WTC_000036699

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NYC-WTC_000036699Source: NYC Law Department, mirrored locally

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