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GCMS blank analysis results, Feb 4, 2002

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank run performed on February 4, 2002, to verify absence of contamination.

NYC-WTC_000016375–000016382

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02

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Scanned page image, NYC-WTC_000016379
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\ JAN0802\LBC.D Vial: 4 Acq On 9 Jan 2002 4:40 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.470 260 264 296 rBV 309561 931079 12.58% 2.517% 2 11.528 701 706 723 rBV 2248969 5600187 75.68% 15.139% 3 15.127 1092 1098 1115 rBV 3426951 7147517 96.60% 19.322% 4 20.396 1665 1672 1695 rBV 3405161 7399405 100.00% 20.003% 5 24.812 2146 2153 2165 rBV2 3246346 7032844 95.05% 19.012%

6 29.888 2701 2706 2714 rVB 338983 673870 9.11% 1.822% 7 32.835 3021 3027 3049 rBV2 2106952 4890904 66.10% 13.221% 8 36.911 3463 3471 3492 rBV2 1176343 3316347 44.82% 8.965%

Sum of corrected areas: 36992153

LBC.D GCMS0103.M Wed Feb 06 11:25:21 2002

NYC-WTC_000016379

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NYC-WTC_000016379Source: NYC Law Department, mirrored locally

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