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GCMS analysis comments for sample AD29466 re-analysis required, Jan 2002

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.

NYC-WTC_000036614–000036644

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 8 Jan 2002 5:14 pm Data File: C:\HPCHEM\1\DATA\JAN0802\29466.D Name: Mise : Method: C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

1-Butanol , 2,2 -dimet 7.48 3.3 ug/1 1401000 ISTD01 11.53 8371950 20.0 Cyclotetrasiloxane , 11.00 9.3 ug/1 3893500 ISTD01 11.53 8371950 2 0.0 Pentane , 2,2,3,4 -1et 12.36 3.9 ug/1 1651150 ISTD01 11.53 8371950 20.0 Heptane 12.80 3.5 ug/1 1458800 ISTD01 11.53 8371950 20.0 Cyslepent as il oxane, 14.17 21.8 ug/1 10149900 ISTD02 15.13 9331300 20.0 2H—1,4-Benzodiazepin 17.31 30.7 ug/1 14317900 ISTD02 15.13 9331300 20.0 Trisiloxane , 1,1,1,5 20.13 24.8 ug/1 12438000 ISTD03 20.40 10020400 20.0 Benzoic acid, 4-etho 20.85 3.7 ug/1 1834770 ISTD03 20.40 10020400 20.0 Benzeneethanamine, N 22.64 13.8 ug/1 10575000 ISTD04 24.81 15379900 20.0 3-1sopropoxy- 1,1,1,7 26.74 9.2 ug/1 7100080 ISTD04 24.81 15379900 20.0 3 -Isopropoxy- 1,1,1,7 28.50 8.5 ug/1 6565720 ISTD04 24.81 15379900 20.0 3 - Isopropoxy -1,1,1,7 30.09 19.7 ug/1 6354560 ISTD05 32.84 6459050 20.0 1 -Menelinoleoylglyce 31.56 19.7 ug/1 6376990 ISTD05 32.84 6459050 20.0 3 - Isopropoxy- 1,1,1,7 32.94 20.1 ug/1 6503570 ISTD05 32.84 6459050 20.0 Ethanedioic acid, bi 34.22 18.2 ug/1 5866390 ISTD05 32.84 6459050 20.0 l - Monolino 1 e oy l g l y c e 35.42 22.0 ug/1 4782530 ISTD06 36.91 4345920 20.0 l - Monolino 1 e oy l g 1 y c e 36.56 15.8 ug/1 3436580 ISTD06 36.91 4345920 20.0 1-Monolinoleoylglyce 37.82 9.9 ug/1 2158900 ISTD06 36.91 4345920 20.0 Trisiloxane , 1,1,1,5 3 9.34 5.7 ug/1 1244270 ISTD06 36.91 4345920 20.0 1 -Monolinoleoylglyce 41.22 3.3 ug/1 714349 ISTD06 36.91 4345920 20.0

29466.D GCMS0103.M Wed Jan 09 16:17:23 2002

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NYC-WTC_000036644

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NYC-WTC_000036644Source: NYC Law Department, mirrored locally

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