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GCMS analytical comments for sample AD30986, Jan 2002

Machine-extracted title · confidence 100%

Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.

NYC-WTC_000018287–000018315

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 18 Jan 2002 5:36 pm Data File: C:\HPCHEM\1\DATA\JAN1802\30986A.D Name: Mise: Method: C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Heptane, 2,4-dimethy 7.01 0.4 ug/1 146813 ISTD01 11.49 7619600 20.0 Silane, tetramethyl- 7.42 3.4 ug/1 1301100 ISTD01 11.49 7619600 20.0 2,4-Dime thy1 -1 - hept e 7.49 1.7 ug/1 631552 ISTD01 11.49 7619600 20.0 Cyolotetrasiloxane, 10.97 2.4 ug/1 910934 ISTD01 11.49 7619600 20.0 Octane, 2,2,6 - trimet 11.64 0.5 ug/1 192115 ISTD01 11.49 7619600 20.0 Hexane, 2,2,5,5-tetr 12.33 0.6 ug/1 227247 ISTD01 11.49 7619600 20.0 Tetracont ane, 3,5,24 12.78 0.5 ug/1 175809 ISTDOl 11.49 7619600 20.0 Cyelopentasiloxane, 14.14 3.7 ug/1 1782760 ISTD02 15.09 9532350 20.0 Cyolohexas iloxane, d 17.27 5.9 ug/1 2825360 ISTD02 15.09 9532350 20.0 propoxy- 1, 1,1,7 20.09 4.2 ug/1 2129950 ISTD03 20.36 10069800 20.0 B icacid, 4-etho 20.82 0.6 ug/1 294085 ISTD03 20.36 10069800 20.0 Benzeneethanamine, N 22.61 2.7 ug/1 1440780 ISTD04 24.78 10664500 20.0 3 -Isopropoxy- 1, 1,1,7 26.70 1.5 ug/1 796299 ISTD04 24.78 10664500 20.0 1 ,^2^, 7 ,7,7 -Heptam 28.47 1.3 ug/1 679000 ISTD04 24.78 10664500 20.0 1-Monolinoleoylglyce 30.06 1.7 ug/1 665348 ISTD05 32.81 7747660 20.0 1 -Monelinoleoylglyce 31.53 1.7 ug/1 639635 ISTD05 32.81 7747660 20.0 Ethanedioic acid, bi 32.91 2.1 ug/1 808955 ISTD05 32.81 7747660 20.0 l -Monelinoleoylglyce 34.19 1.4 ug/1 545671 ISTD05 32.81 7747660 20.0 3-. roboXY-1,1,1,7 35.39 1.2 ug/1 386820 ISTD06 36.87 63'29060 20.0 2- oxyphenyl pyruv 36.52 0.7 ug/1 209039 ISTD06 36.87 6329060 20.0

30986A.D GCMS1126.M Tue Jan 22 10:18:55 2002

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NYC-WTC_000018315

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NYC-WTC_000018315Source: NYC Law Department, mirrored locally

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