Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
NYC-WTC_000033911–000033935Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Tentatively Identified Compound (LSC) summary
Operator ID: 209 GALOS Date Acquired: 8 Jan 2002 4:16 pm Data File: C:\HPCHEM\1\DATA\JAN0802\28327.D Name: 508 Mise: Method: C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L
TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc
1,4-Dichl orobenzene - 11.39 0.5 ug/1 186325 ISTD01 11.53 7182770 20.0 Cyelopent a s i l oxane, 14.16 2.3 ug/1 1064210 ISTD02 15.13 9364450 20.0 1-1,1,5,7,7,7-Heptam 17.30 9.3 ug/1 4344880 ISTD02 15.13 9364450 20.0 2 -Propanone, 1 - (1 - me 18.00 1.0 ug/1 476234 ISTD03 20.40 9975640 20.0 3—Isopropoxy- 1,1,1,7 20.12 8.2 ug/1 4068410 ISTD03 20.40 9975640 20.0 Phenol, 2,4-bis(1,1- 20.57 0.5 ug/1 234380 ISTD03 20.40 9975640 20.0 Benzoic acid, 4-etho 20.85 3.4 ug/1 1712470 ISTD03 20.40 9975640 20.0 N—(Trifluoracety1) -0 22.64 5.3 ug/1 2929170 ISTD04 24.81 11135400 20.0 3 -Isopropoxy- 1,1,1,7 26.73 2.9 ug/1 1594840 ISTD04 24.81 11135400 20.0 N—Trifluoroacetyl) - 28.50 2.3 ug/1 1299810 ISTD04 24.81 11135400 20.0 1,11.5,7,7,7 -Heptam 30.09 3.4 ug/1 1153680 ISTD05 32.85 6723050 20.0 l -Monolinoleoylglyce 31.56 3.0 ug/1 1015720 ISTD05 32.85 6723050 20.0 1 -Monolinoleoylglyce 32.94 3.0 ug/1 1015960 ISTD05 32.85 6723050 20.0 3 - Isopropoxy- 1,1,1,7 34.22 2.1 ug/1 705173 ISTD05 32.85 6723050 20.0 1-Monolinoleoylglyce 35.43 1.9 ug/1 453817 ISTD06 36.91 4738380 20.0 1 -Monolinoleoylglyce 36.55 1.1 ug/1 262151 ISTD06 36.91 4738380 20.0 3 - Isepropoxy- 1,1,1,7 37.82 0.6 ug/1 137729 ISTD06 36.91 4738380 20.0
28327.D GCMS1126.M Wed Jan 09 09:15:59 2002
NYC-WTC_000033935
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NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder