GCMS blank analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1301\LB.D Vial: 4 Acq On : 13 Dec 2001 12:47 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.72 ug/1 210056 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-ethoxy-l-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1- (2-methoxypropoxy) - 148 C7H16O3 013429-07-7 50 3 2-Propanol, 1, Z’ -oxybis- 134 C6H14O3 000110-98-5 50 4 2-Butanol, 3,8 '-oxybis- 162 C8H18O3 054305-61-2 50 'Abundance Scan 695 (11.427 min): LB.D (-) m/z 59.05 100.00% I 59

i 5000-

— 45

-4+ 73

87 ■ i ■ ■ ■■ ■ i • ■ 103 N 11.00 11.20 11.40 11.60 11.80 m/z 44.95 51.80% miz-> 30 40 50 70 60 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy)- 59

i I

m/z-s 5000

‘Abundance - 30 31

40 45 73 103 i

........, ........................... ..........4.................... 130 50 60 59 70 80 90 100 110 #9233; 2-Propanol, 1-(2-methoxypropoxy)- 120 130 _N . —_ TI 11.00 11.20 11.40 11.60 11.80

11.00 11.20 11.40 11.60 11.80 5000- m/z 73.00 27.20%

31 45 73 II . I■ • I • ' l 1 ■ I ■ ■ ■ ■ l ■ • ■ • I ■ 14-130 m/z-> 30 40 50 60 70 80 90___ 100 110 120 130 Abundance i #6087: 2-Propanol, 1,1'-oxybis- TTIfTT 1............ .... । । > > i 59 11.00 11.20 11.40 11.60 11 80 m/z 41.05 24.18%

Ik 31 5000 45 103

' ' I ' ' ' ' I 1 1——,|.i ..... 72....... 89 1 I' ■ ■ ■ i 1 ■ ■ ■ i' ■ '■i■ —MPMS-r miz-> 30 40 50 I60 70 80 90 100 110 120 130 11.00 11.20 11:40 11.60 11.80

LB.D GCMS1126.M Fri Dec 21 13:17:47 2001 Page 3

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