GCMS analysis comments, sample AD29524, January 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\29520.D Vial: 7 Acq On : 13 Dec 2001 3:43 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.33 2.33 ug/1 901705 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-l-methylet 148 C7H16O3 020324-32-7 78 2 2-Butanol, 3,3 %-oxybis- - 162 C8H18O3 054305-61-2 64 3 2-Propanol, l/l'-oxybis- 134 C6H14O3 000110-98-5 56 4 2-Propanol, J-(2-methoxypropoxy)- . 148 C7H1603 013429-07-7 50 Abundance' 4 Scan 684 (11.327 min): 29520.D (-) m/z 59.05 100.00% 59

5000

39 II -----PP TT 45 73

—9—+ 103

........ 130.... .M 11.00 m/z 11.20 44.95, 11.40 11.60 47.81% "I

miz-> 20 30 40 50 70 60 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59 V 5000 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 33.48% --H — m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 59 • i • • TI 11.00 11.20 11.40 11.60 5000 31 45 m/z 73.00 27.71% 103 i . : i I 134 1 I ' 1 1 1 I ' ' ‘ ' I ' ' m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1’-oxybis- TIT ' 1 I 59 11.00 11.20 11.40 11.60 m/ z 41.05 24.88% 31 5000- 45

103 — — i ' . 89 V m/z-> 20 30 40 50 Hr 72 — I ' i 1 ■ • • i "L." ' I 1 1 1 । I ————— 11111r J 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29520.D GCMS1126.M Fri Dec 21 13:14:08 2001 Page 2

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