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GCMS analysis results sample AD29299, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29299 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036403–000036413

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC12O1\29299 .D Vial: 29 Acq On 13 Dec 2001 5:18 am Operator: 209 GALOS Sample gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 10:42 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1011928 • 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3870440 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.56 164 1925332 20.00 ug/1 -0.02 29) Phenanthrene-dlO 24.97 . 188 2787547 20.00 ug/1 -0.02 38) Chrysene-dl2 33.00 240 1707585 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 1118898 20.0C ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 201620 6.08 ug/mL -0.02 Spiked Amount 5.000 Recovery = 121.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.21 74 358 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.04 77 397 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene , 15.33 128 1446 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. • 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.17 165 354 N.D. 25) Diethylphthalate 22.11 149 461 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29299.D GCMS1126.M Fri Dec 21 12:54:33 2001 Page 1

NYC-WTC_000036405

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NYC-WTC_000036405Source: NYC Law Department, mirrored locally

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