NYC-WTC_000036350
Blank sample analysis report for GCMS testing showing non-detect levels for target analytes.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 12 pages
GCMS blank results for sample AD29022, Dec 17 2001
Machine-extracted title · confidence 95%Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
NYC-WTC_000035776–000035787Folder label: “GCMS X 11/30/01 A 12/10/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1001\LB.D Vial: 3 Acq On : 10 Dec 2001 11:42 am Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:18 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 827694 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3181409 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1585058 20.00 ug/1 -0.02 2 9) Phenanthrene-dl0 24.97 188 2266491 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1350464 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 934892 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 145151 5.38 ug/mL -0.02 Spiked Amount 5.000 Recovery = 107.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.13 74 1425 N.D. 3) bis(2-Chloroethyl)ether 11.01 93 368 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2' -oxybis (1 -Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.03 77 105 N.D. 12) 1sophorone 13.50 82 178 N.D. 13) bis(2-Chloroethoxy)methane 14.55 93 221 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1367 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 20.10 152 190 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.00 165 286 N.D. 25) Diethylphthalate 22.07 149 2490 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 22.68 77 3363 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS1126.M Wed Dec 12 15:19:07 2001 Page 1
NYC-WTC_000035777
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NYC-WTC_000004149
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