GCMS analysis comments for sample AD29188, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29188 indicate no unusual compounds detected except for unknowns and Sur_2,4-DDD.

NYC-WTC_000035798–000035807

Folder label: “GCMS X 11/30/01 A 12/10/01”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1001\29188.D Vial: 5 Acq On : 10 Dec 2001 2:38 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:06 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 827936 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3144517 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.55 164 1591772 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2222358 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1319796 20.00 ug/1 -0.02 44) Perylene-dl2 37.09 264 886495 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 148574 5.62 ug/mL -0.02 Spiked Amount 5.000 Recovery = 112.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.13 74 699 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.07 77 272 N.D. 12) isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1887 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Ac enapht hene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.29 165 355 N.D. 25) Diethylphthalate 22.07 149 1685 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.72 77 358 N.D.

(#) = qualifier out of range (m) = manual integration 29188.D GCMS1126.M Thu Dec 13 10:06:32 2001 Page 1

NYC-WTC_000035800

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000035800Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis comments for sample AD29134, Dec 17 2001 · Box DEP Box 22

NYC-WTC_000035865

Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.

Same agency, volume and box · similarity 0.998