Laboratory notes indicating re-extraction is required due to low recovery and potential contamination.
NYC-WTC_000035745–000035754Folder label: “GCMS X 11/28/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data' File C: \HPCHEM\ 1 \DATA\DEC0 601\28861.D Vial: 37 Acq On 7 Dec 2001 10:49 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 11 15:46 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 19.94 163 293 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 20.65 153 122 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.02 65 335 N.D. 37) 2,4-Dinitrotoluene 21.22 165 188 N.D. 38) Diethylphthalate 22.07 149 1071 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 4 0) Fluorene 22.18 166 190 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.69 77 290 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.04 178 787 N.D. 49) Anthracene 25.17 178 632 N.D. 50) Di-n-butylphthalate 26.99 149 14914 N.D. 51) Fluoranthene 28.68 202 240 N.D. 54) Pyrene 29.33 202 229 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 56) Benzo(a)anthracene 33.01 228 5803 N.D. 57) Bis(2-ethylhexyl)phthalate 33.29 149 5156 N.D. 58) Chrysene 33.09 228 585 N.D. 60) Di-n-Octylphthalate 35.02 149 101 N.D. 61) Benzo(b)fluoranthene 36.05 252 341 N.D. 62) Benzo(k)fluoranthene 36.05 252 342 N.D. 63) Benzo(a)pyrene 37.11 252 5749 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.
(#) = qualifier out of range (m) = manual integration 28861.D GCMS1126.M Wed Dec 12 10:12:15 2001 Page 2
NYC-WTC_000035748
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NYC-WTC_000035755
Lab report noting bis(2-Ethylhexyl) Sebacate detection and potential laboratory contamination in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035717
Laboratory notes identifying potential laboratory contamination by specific esters in sample AD28899.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035990
Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in sample AD29028 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035727
Laboratory notes stating the GCMS scan of sample AD28897 revealed no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035909
Lab notes for sample AD29024 indicate detection of bis(2-Ethylhexyl)phthalate and no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035843
Lab notes for sample AD29190 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036000
Analysis comments for sample AD29089 reporting no unusual compounds in GCMS scan but noting one compound recovery above acceptance range in LCS Standard.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035967
Laboratory report documenting GCMS scan results for sample AD29138 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035505
Gas chromatography-mass spectrometry analysis results for sample AD28859 showing bis(2-Ethylhexyl)phthalate presence at 0.81 ug/L with quality control notes on LCS standard recover
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036425
Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033874
Laboratory report detailing GCMS scan results and recovery rates for environmental sample AD28147 analyzed in December 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019070
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30115 conducted on January 9, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000035662
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035663
Fragmented document containing method 508 data and sample IDs processed by GCMS in late 2001.
Filed in the same folder
NYC-WTC_000035664
Laboratory data sheet recording GCMS Method 508 analysis of a blank sample for nitrosamines and chlorinated compounds.
Filed in the same folder
NYC-WTC_000035674
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035678
Document containing calculated reference values for various organic compounds analyzed by GCMS.
Filed in the same folder