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GCMS analysis comments, sample AD28857, Dec 2001

Machine-extracted title · confidence 95%

GCMS scan results for sample AD28857 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate and noting low pH.

NYC-WTC_000035489–000035496

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC0601\28857.D Vial: 30 Acq On : 7 Dec 2001 3:58 am Operator: 209 GALOS Sample : 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 11 12:06 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 0.00 163 0 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 33) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.10 65 498 N.D. 37) 2,4-Dinitrotoluene 21.22 165 317 N.D. 38) Diethylphthalate 22.07 149 2768 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 4 0) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.57 77 122 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 4 6) Hexachiorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 24.97 178 973 N.D. 49) Anthracene 24.97 178 973 N.D. 50) Di-n-butylphthalate 26.98 149 18892 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.49 149 491 N.D. 56) Benzo(a)anthracene 33.01 228 4384 N.D. 57) Bis(2-ethylhexyl)phthalate 33.29 149 38680 0.37 ug/1 97 58) Chrysene 33.01 228 4384 N.D. 60) Di-n-Octylphthalate 35.04 149 798 N.D. 61) Benzo(b)fluoranthene 36.12 252 181 N.D. 62) Benzo(k)fluoranthene 36.12 252 181 N.D. 6 3) Benzo(a)pyrene 37.09 252 4483 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28857.D GCMS1126.M Tue Dec 11 15:40:09 2001 Page 2

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