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GCMS analysis comments for sample AD28758, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in a WTC environmental sample.

NYC-WTC_000035314–000035321

Folder label: “GCMS X 11/26/01 A 12/6/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC0501\28758.D Vial: 15 Acq On : 6 Dec 2001 2:17 am Operator: 209 GALOS Sample : 11/26 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 6 3:05 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 0.00 163 0 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. 3 3) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 • N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.29 165 185 N.D. 38) Diethylphthalate 22.11 149 1360 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 4 0) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-DiphenyIhyd 23.10 77 209 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.01 178 911 N.D. 49) Anthracene 25.01 178 911 N.D. 50) Di-n-butylphthalate 27.01 149 10993 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.52 149 1652 N.D. 56) Benzo(a)anthracene 33.04 228 4206 N.D. 57) Bis(2-ethylhexyl)phthalate 33.32 149 30654 0.29 ug/1 95 58) Chrysene 33.04 228 4206 N.D. 60) Di-n-Octylphthalate 0.00 149 0 N.D. 61) Benzo(b)fluoranthene 0.00 252 0 N.D. 62) Benzo(k)fluoranthene 0.00 252 0 N.D. 63) Benzo(a)pyrene 37.13 252 4479 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo (g, h, i) perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28758.D GCMS1126.M Fri Dec 07 15:07:18 2001 Page 2

NYC-WTC_000035317

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NYC-WTC_000035317Source: NYC Law Department, mirrored locally

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