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GCMS comments for sample AD28902, Dec 17 2001

Machine-extracted title · confidence 90%

Laboratory notes stating the GCMS scan of sample AD28902 revealed no unusual compounds.

NYC-WTC_000035692–000035699

Folder label: “GCMS X 11/28/01 A 12/7/01

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Scanned page image, NYC-WTC_000035697
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\28902 .D Vial: 8 Acq On 6 Dec 2001 8:10 pm Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.676 716 722 742 rBV 1897267 5476966 71.90% 14.224% 2 15.275 1109 1114 1133 rBV 3282143 7124843 93.53% 18.504% 3 20.553 1683 1689 1711 rBV 3536406 7617687 100.00% 19.784% 4 24.978 2164 2171 2182 rBV2 3262989 7172261 94.15% 18.627% 5 25.116 2183 2186 2197 rVB 28904 84227 1.11% 0.219%

6 30.055 2718 2724 2732 rBV 340813 685250 9.00% 1.780% 7 33.011 3039 3046 3061 rBV2 2344673 5549507 72.85% 14.413% 8 37.106 3483 3492 3514 rBV2 1697775 4793908 62.93% 12.450%

Sum of corrected areas: 38504649

28902.D GCMS1126.M Tue Dec 11 16:09:17 2001

NYC-WTC_000035697

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NYC-WTC_000035697Source: NYC Law Department, mirrored locally

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