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Document / 11 pages

GCMS analysis comments, sample AD28967, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.

NYC-WTC_000035607–000035617

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC0701\28967.D Vial: 13 Acq On 8 Dec 2001 2:38 am Operator: 209 GALOS Sample : 11/29 gc/ms scan Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integ rator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 7.602 275 279 293 rBV 432007 1040149 14.04% 2.677% 2 11.339 682 686 691 rBV 101901 213468 2.88% 0.549% 3 11.421 691 695 711 rVB 112263 300299 4.05% 0.773% 4 11.669 715 722 740 rBV 2208927 5314102 71.71% 13.676% 5 15.277 1109 1115 1133 rBV 3120625 6706921 90.51% 17.260%

6 20.556 1683 1690 1713 rBV 3334235 7410157 100.00% 19.070% 7 24.972 2165 2171 2183 rBV2 3066880 7060415 95.28% 18.170% 8 25.118 2183 2187 2198 rVB2 28940 93366 1.26% 0.240% 9 30.048 2719 2724 2732 rBV 462776 964900 13.02% 2.483% 10 33.014 3040 3047 3066 rBV2 2272670 5407340 72.97% 13.915%

11 33.289 3072 3077 3093 rVB 43430 136199 1.84% 0.351% 12 37.099 3484 3492 3506 rBV2 1445018 4211120 56.83% 10.837%

Sum of corrected areas: 38858436

28967.D GCMS1126.M Thu Dec 13 10:22:05 2001

NYC-WTC 000035612

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NYC-WTC_000035612Source: NYC Law Department, mirrored locally

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