NYC-WTC_000034971
Blank test results confirming no detectable contaminants above method detection limits for sample AD28662.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 34 pages
GCMS analysis comments for sample AD28689, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28689.
NYC-WTC_000035195–000035228Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report
»Data File C: \HPCHEM\1\DATA\DEC0401\28689.D Vial: 14 Acq On ,5 Dec 2001 1:04 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
41.55 1.98 ug/1 293324 Perylene-d12 37.13
Hit# of Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 Cyclo; opanamine, N-methyl-1-phenyl 147 C10H13N 056771-48-3 27 3 3,6-Dzoxa-2,4,5,7-tetrasilaoctane, 294 C10H30O2S14 004342-25-0 16 4 But a: dioic acid,bis(trimethylsily 262 C10H2204Si2 _ 040309-57-7 16 Abundance Scan 3977 (41.554 min): 28689.D (-) m/ z 73.00 100.00% 73 147
221 5000- 281 355
TITmTt XL . .. H.... “ TWTTUTTTTTTT m/z 147.00 ''1' 39 mm 97 117 177 .1 1 L 327 J. 401 429 41.20 4140 41.60 41.80 83.2 9% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, i,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
5000- TI 281 41.20 41.40 41.60 41.80 45 369 54.31% 207 1 1........ 117..... ............. — 249 . " ’ ■ i ■' " 1 p i r.111111111111 n 1111111111111 > 11 TCTTgg mmmpmpm miz-> 40 60 80 100120140160180200220240260280300320340 360380400420 Abundance — 10J. C yelepropanamine. N-methyl-1-phenyf- 147
41.20 41.40 41.60 41.80_____ 5000 m/z 281.00 34.24% 42 .649220 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420' miz-> Abundance #41682:3>6-Dioxa-2,4,5,7-tetrasi(aoctane. 2.2,4,4,5,5,7,7-
A LI—E—EI—UTLIIEET"IEEIT 147 221 41.20 41.40 41.60 41.80 m/z 355.00 25.34% 73 5000 191 117 279
miz-> 40 60 80 10012014016018020022024026028030032034036 0380400420 41.20 41.40 41.60 41.80
28689.D GCMS1126.M Mon Dec 10 10:20:08 2001 Page 15
NYC-WTC_000035216
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