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GCMS analysis comments for sample AD28688, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting di-n-butylphthalate detection and TurboVap contamination with recovery data for sample AD28688.

NYC-WTC_000035026–000035043

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DECO401\28688.D Vial: 6 Acq On 4 Dec 2001 5:15 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 18:04 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Conc Unit Qvalue

33) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.20 65 360 N.D. 37) 2,4-Dinitrotoluene 21.01 165 210 N.D. 38) Diethylphthalate 22.10 149 1316 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D: 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.02 178 812 N.D. 49) Anthracene 25.02 178 812 N.D. 50) Di-n-butylphthalate 27.02 149 42963 0.30 ug/l 99 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.56 149 499 N.D. 56) Benzo(a)anthracene 33.03 228 3243 N.D. 57) Bis(2-ethylhexyl)phthalate. 33.31 149 12392 N.D. 58) Chrysene 33.03 228 3243 N.D. 60) Di-n-Octylphthalate 35.08 149 291 N.D. 61) Benzo(b)fluoranthene 36.10 252 400 N.D. 62) Benzo(k)fluoranthene 36.10 252 400 N.D. 63) Benzo(a)pyrene 37.12 252 3474 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 28688.D GCMS1126.M Thu Dec 06 13:02:06 2001 Page 2

NYC-WTC 000035028

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NYC-WTC_000035028Source: NYC Law Department, mirrored locally

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