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GCMS calibration results for sample AD28662, Dec 2001

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Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.

NYC-WTC_000034958–000034970

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Dta File : C:\HPCHEM\l\DATA\DEC0401\LB.D Vial: 3 Acq On : 4 Dec 2001 2:19 pm Operator: 209 GALOS : Sample : 1b 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 6 12:29 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.15 152 606 N.D. 3 4) Acenaphthene 20.68 153 800 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. d 37) 2,4-Dinitrotoluene 21.21 165 400 N.D. 38) Diethylphthalate 22.10 149 1491 N.D. 39) 4-Chlorophenyl-phenylether 22.25 204 182 N.D. 40) Fluorene 22.21 166 632 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.07 178 1866 N.D. 49) Anthracene 25.22 178 600 N.D. 50) Di-n-butylphthalate 27.01 149 6108 N.D. 51) Fluoranthene 28.70 202 627 N.D. > 54) Pyrene 29.38 202 343 N.D. 55) Butylbenzylphthalate 31.72 149 697 N.D. 5 6) Benzo(a)anthracene 33.04 228 3649 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 3183 N.D. 58) Chrysene 33.10 228 1164 N.D. 60) Di-n-Octylphthalate 35.05 149 171 N.D. 61) Benzo(b)fluoranthene 36.09 252 560 N.D. 62) Benzo(k)fluoranthene 36.15 252 1488 N.D. 63) Benzo(a)pyrene 36.97 252 319 N.D. 64) Indeno(1,2, 3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS1126.M Thu Dec 06 12:30:20 2001 Page 2

NYC-WTC_000034960

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NYC-WTC_000034960Source: NYC Law Department, mirrored locally

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