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← Document results/DEP Box 22/GCMS X 11/23/01 A 11/29/01
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GCMS analysis comments for sample AD28651, Dec 2001

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Laboratory report detailing GCMS scan results for sample AD28651, noting low pH and recovery rates.

NYC-WTC_000034938–000034945

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\DEC0601\28650.D Vial: 4 Acq On : 6 Dec 2001 2:04 pm Operator: 209 GALOS Sample : re extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 6 15:04 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 33) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.13 65 527 N.D. 37) 2,4-Dinitrotoluene 21.42 165 300 N.D. 38) Diethylphthalate 22.07 149 2553 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.66 77 120 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.04 178 796 N.D. 49) Anthracene 25.04 178 796 N.D. 50) Di-n-butylphthalate 27.00 149 32772 N.D. 51) Fluoranthene 0.00 202 0 N.D. s 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.49 149 753 N.D. 56) Benzo(a)anthracene 33.01 228 6695 N.D. 57) Bis(2-ethylhexyl)phthalate 33.29 149 40505 0.33 ug/1 98 58) Chrysene 33.09 228 1203 N.D. 60) Di-n-Octylphthalate 35.02 149 1515 N.D. 61) Benzo(b)fluoranthene 36.04 252 1976 N.D. 62) Benzo(k)fluoranthene 36.11 252 2362 N.D. 63) Benzo(a)pyrene 36.94 252 1469 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 41.88 276 100 N.D.

(#) = qualifier out of range (m) = manual integration 28650.D GCMS1126.M Thu Dec 06 15:04:57 2001 Page 2

NYC-WTC_000034940

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NYC-WTC_000034940Source: NYC Law Department, mirrored locally

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