Gas chromatography-mass spectrometry analysis of sample AD28432 conducted November 30, 2001, detecting other unknown compounds with results referenced in comments.
NYC-WTC_000034289–000034301Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC0501\28432 .D Vial: 4 Acq On : 5 Dec 2001 3:34 pm Operator: 209 GALOS Sample : re extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 5 16:23 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.18 165 203 • N.D. 38) Diethylphthalate 22.10 149 722 • N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 4 7) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.08 178 224 / N.D. 49) Anthracene 25.08 178 224 / N.D. 50) Di-n-butylphthalate 27.01 149 9851 / N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 56) Benzo(a)anthracene 33.04 228 3412 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 4200 N.D. 58) Chrysene 33.04 228 3412 N.D. 60) Di-n-Octylphthalate 35.50 149 100 N.D. 61) Benzo(b)fluoranthene 0.00 252 0 N.D. 6 2) Benzo(k)fluoranthene 0.00 252 0 N.D. 63) Benzo(a)pyrene 37.13 252 3844 N.D. 64) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.
(#) = qualifier out of range (m) = manual integration 28432.D GCMS1126.M Thu Dec 06 11:03:14 2001 Page 2
NYC-WTC_000034292
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NYC-WTC_000034235
Laboratory commentary noting moderate recovery rates and absence of unusual compounds in sample AD28273.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034258
Laboratory report documenting GCMS analysis of sample AD28473 conducted between November 21 and 26, 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036184
Follow-up report documenting re-extraction of sample AD29232 which maintained low recovery rates despite re-processing.
Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034938
Laboratory report detailing GCMS scan results for sample AD28651, noting low pH and recovery rates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034741
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035000
Laboratory report detailing GCMS scan results for sample AD28680, noting phthalate detection and recovery rates.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036000
Analysis comments for sample AD29089 reporting no unusual compounds in GCMS scan but noting one compound recovery above acceptance range in LCS Standard.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036425
Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034790
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28599 analyzed in early December 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033874
Laboratory report detailing GCMS scan results and recovery rates for environmental sample AD28147 analyzed in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033856
Analytical commentary for sample AD28141 dated December 6, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033865
Gas chromatography-mass spectrometry analysis of sample AD28141 showing no unusual compounds detected; method acceptance ranges to be established and used.
1 shared non-person entities · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder