Gas chromatography-mass spectrometry analysis of sample AD28432 conducted November 30, 2001, detecting other unknown compounds with results referenced in comments.
NYC-WTC_000034289–000034301Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC 0501\28432.D Vial: 4 Acq On : 5 Dec 2001 3:34 pm Operator: 209 GALOS Sample : re extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 5 16:23 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 842102 20.00 ug/1 0.01 15) Naphthalene-d8 15.32 136 3155400 20.00 ug/1 0.01 26) Acenaphthene-diO 20.59 164 1548029 20.00 ug/1 0.01 42) Phenanthrene-diO 25.00 188 2179835 20.00 ug/1 0.01 53) Chrysene-dl2 33.04 240 1379065 20.00 ug/1 0.00 59) Perylene-dl2 37.13 264 944225 20.00 ug/1 0.01 System Monitoring Compounds 52) 2,4-DDD 30.08 235 107725 4.15 ug/mL 0.01 Spiked Amount 5.000 Recovery = 83.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.13 74 1074 N.D. 4) Phenol 11.20 94 N.D. 5) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 6) 2-Chlorophenol 0.00 128 0 N.D. 7) 1,3-Dichlorobenzene 0.00 146 0 N.D. 8) 1,4-Dichlorobenzene 0.00 146 0 N.D. 9) 1,2-Dichlorobenzene 0.00 146 0 N.D. 10) 2-Methylphenol 0.00 108 0 N.D. 11) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 12) 3&4-Methylphenol 0.00 108 0 N.D. 13) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 14) Hexachloroethane 0.00 117 0 N.D. 16) Nitrobenzene 0.00 77 0 N.D. 17) Isophorone 0.00 82 0 N.D. 18) 2-Nitrophenol 0.00 139 0 N.D. 19) 2,4-Dimethylphenol 0.00 107 0 N.D. 20) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 3) Naphthalene 15.36 128 1127 N.D. 24) Hexachlorobutadiene 0.00 225 0 N.D. 25) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 27) Hexachlorocyclopentadiene 0.00 237 0 N.D. 28) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 0.00 163 0 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. (#) = qualifier out of range (m) = manual integration 28432.D GCMS1126.M Thu Dec 06 11:03:10 2001 Page 1
NYC-WTC_000034291
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NYC-WTC_000034235
Laboratory commentary noting moderate recovery rates and absence of unusual compounds in sample AD28273.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034258
Laboratory report documenting GCMS analysis of sample AD28473 conducted between November 21 and 26, 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036184
Follow-up report documenting re-extraction of sample AD29232 which maintained low recovery rates despite re-processing.
Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034938
Laboratory report detailing GCMS scan results for sample AD28651, noting low pH and recovery rates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034741
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035000
Laboratory report detailing GCMS scan results for sample AD28680, noting phthalate detection and recovery rates.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036000
Analysis comments for sample AD29089 reporting no unusual compounds in GCMS scan but noting one compound recovery above acceptance range in LCS Standard.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036425
Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034790
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28599 analyzed in early December 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033874
Laboratory report detailing GCMS scan results and recovery rates for environmental sample AD28147 analyzed in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033856
Analytical commentary for sample AD28141 dated December 6, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033865
Gas chromatography-mass spectrometry analysis of sample AD28141 showing no unusual compounds detected; method acceptance ranges to be established and used.
1 shared non-person entities · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder