NYC-WTC_000035890
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
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GCMS blank analysis report for sample AD28593, Nov-Dec 2001
Machine-extracted title · confidence 100%Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
NYC-WTC_000034731–000034740Folder label: “GCMS X 11/23/01 A 11/29/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2 6 01\LBC.D Vial: 4 Acq On : 27 Nov 2001 8:13 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 15:06 2001 Quant Results Files GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.69 152 751000 20.00 ug/1 0.00 15) Naphthalene-d8 15.30’ 136 2844617 20.00 ug/1 0.00 26) Acenaphthene-diO 20.57 164 1345165 20.00 ug/1 0.00 42) Phenanthrene-diO 25.00 188 1828041 20.00 ug/1 0.00 53) Chrysene-dl2 33.03 240 907678 20.00 ug/1 0.00 59) Perylene-dl2 37.11 264 578478 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 30.07 235 86194 3.96 ug/mL 0.00 Spiked Amount 5.000 Recovery = 79.20% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.23 74 305 N.D. 4) Phenol 0.00 94 0 N.D. 5) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 6) 2-Chlorophenol 0.00 128 0 N.D. . 7) 1,3-Dichlorobenzene 0.00 146 0 N.D. 8) 1,4-Dichlorobenzene 0.00 146 0 N.D. 9) 1,2-Dichlorobenzene 0.00 146 0 N.D. 10) 2-Methylphenol 0.00 108 0 N.D. 11) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 12) 3&4-Methylphenol 0.00 108 0 N.D. 13) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 14) Hexachloroethane 0.00 117 0 N.D. 16) Nitrobenzene 0.00 77 0 N.D. 17) Isophorone 0.00 82 0 N.D. 18) 2-Nitrophenol 0.00 139 0 N.D. 19) 2,4-Dimethylphenol 0.00 107 0 N.D. 20) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 23) Naphthalene 15.36 128 387 N.D. 24) Hexachlorobutadiene 0.00 225 0 N.D. 25) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 27) Hexachlorocyclopentadiene 0.00 237 0 N.D. 28) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 0.00 163 0 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. d (#) = qualifier out of range (m) = manual integration LBC.D GCMS1126.M Thu Nov 29 15:07:06 2001 Page 1
NYC-WTC_000034732
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NYC-WTC_000016242
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