Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
NYC-WTC_000034160–000034167Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C: \HPCHEM\1 \DATA\NOV2 601 \LBB . D Vial: 23 Acq On : 27 NOV 2001 8:13 am Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 13:30 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 873779 20.00 ug/1 0.00 15) Naphthalene-d8 15.30 136 3257018 20.00 ug/1 0.00 26) Acenaphthene-diO 20.58 164 1536388 20.00 ug/1 0.00 42) Phenanthrene-diO 24.99 188 2045010 20.00 ug/1 0.00 53) Chrysene-dl2 33.03 240 837114 20.00 ug/1 0.00 59) Perylene-dl2 37.11 264 491597 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 30.07 235 54895 2.25 ug/mL 0.00 Spiked Amount 5.000 Recovery = 45.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.20 74 385 / N.D. 4) Phenol 0.00 94 0 N.D. 5) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 6) 2-Chlorophenol 0.00 128 0 N.D. 7) 1,3-Dichlorobenzene 0.00 146 0 N.D. 8) 1,4-Dichlorobenzene 0.00 146 0 N.D. 9) 1,2-Dichlorobenzene 0.00 146 0 N.D. 10) 2-Methylphenol 0.00 108 0 N.D. 11) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 12) 3&4-Methylphenol 0.00 108 0 N.D. 13) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 14) Hexachloroethane 0.00 117 0 N.D. 16) Nitrobenzene 0.00 77 0 N.D. 17) Isophorone 0.00 82 0 N.D. 18) 2-Nitrophenol 0.00 139 0 N.D. 19) 2,4-Dimethylphenol 0.00 107 0 N.D. 20) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 23) Naphthalene 15.35 128 557 N.D. 24) Hexachlorobutadiene 0.00 225 0 N.D. 25) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 27) Hexachlorocyclopentadiene 0.00 237 0 N.D. 28) 2, 4,6-Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 0.00 163 0 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. d (#) = qualifier out of range (m) = manual integration LBB.D GCMS1126.M Fri NOV 30 13:30:23 2001 Page 1
NYC-WTC_000034161
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NYC-WTC_000034731
Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
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GCMS analysis results for sample AD28903 dated December 15, 2001, showing non-detect levels for various compounds.
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Laboratory data sheet recording GCMS Method 508 analysis of a blank sample for nitrosamines and chlorinated compounds.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28667 analyzed in early December 2001.
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Laboratory report detailing GCMS scan results for sample AD28596, noting phthalate detection and recovery rates.
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Laboratory commentary dated December 3, 2001, regarding sample AD28469 analysis, noting bis(2-Ethylhexyl)phthalate presence.
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Laboratory report showing non-detect levels for various volatile organic compounds in a WTC blank sample.
Same agency, volume and box · similarity 0.994
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28668 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.994
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009428
Laboratory data table recording drip rates and volumes for GCMS Method 508 analysis.
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Blank analysis report for DEP sample AE02966 showing all target compounds below minimum detection limits.
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Laboratory report of a GCMS blank run for sample AD31347 performed on February 5, 2002.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
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NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
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NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
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NYC-WTC_000034175
Laboratory report of GCMS reference analysis for sample AD28263 conducted on November 30, 2001.
Filed in the same folder