GCMS comments for sample AD28273, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0501\28273.D Vial: 5 Acq On 5 Dec 2001 4:33 pm Operator 209 GALOS Sample re extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.39 0.52 ug/1 119784 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 59 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 47 4 2-Propanol, 1-(2-ethoxypropoxy)- 162 C8H18O3 010143-32-5 38

N Abundance Scan 691 (11,390 min): 28273.D (-) m/z 59.05 100.00% 59 45 5000 103 73

m/z-> —ill 30 40 ■ i ■ — ■ ■ ■ ■ i #

50 60 70 80 84 । TIT m-p-m ! T H-r-j n TT T r-i . TT . T 90 100 110 120 130 11.00 11.20 11.40 11.60 11.80 m/z 45.05 54.06%

NA Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 1 I 1 ' ' 1 I ' , |T-T --T n 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 102.95 39.40%

miz-> ■ ■ — . 111. ।. 11. ■ I

30 40 50 ITT Tur.'.'.T ' I60 70 80 90 T100 110 120 130 130 Abundance #6086:1-Propanol, 2-(2-hydroxypropoxy)- 59 1 I 1 1 1 • i 1 1 f 11.00 11.20 11.40 11.60 11.80 5000 m/ Z 73.00. 28.22%

11 31 45 103

75 89 1 1 i 1 111 1 4— 1 — —+Tr m/z-> 30 40 50 (60 70 80 90 100 110 120 130 Abundance #9233:2-Propanol, 1-(2-methoxypropoxy)- 59 —IPT * I 1 1 ‘ 1 I 1 ’ 1 1 I ' '

_ NA 11.00 11.20 11.40 11.60 11.80 m/z 41.05 27.05% 5000

31 45 - 73 104 m/z—> 30 40 50 60 --- 70 80 90 100 110 120 130 130 -Aal —M—A 11.00 11.20 11.40 11.60 11.80

28273.D GCMS1126.M Thu Dec 06 08:51:45 2001 Page 2

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