Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
NYC-WTC_000034180–000034197Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28263.D Vial: 33 Acq On : 29 Nov 2001 6:28 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,2-Benzenedicarboxylic acid, Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
39.60 4.84 ug/1 718488 Perylene-d12 37.12
Hit# of 5 Tentative/ID MW MolForm CAS# Qual
1 1,2 -Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 25 2 N-Benzhydryli e-1-(2,4,6-trimethy 343 C24H25NO 089839-57-6 22 3 1,2-Bis (trime hylsiloxy) ethane 206 C8H2202Si2 007381-30-8 16 4 Ethanedioi acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 16 Abundance A. Scan 3764 (39.596 min): 28263.D (-) m/z 73.00 100.00% 73 147 221 5000 281 355
m/z-> 39 , 96 117 J 191 T TT TTTTTTTTT rtr 4 mmmm 40 60 80 100120140160180200220240260280300320340360380400420 2533 L TTTT 3271 39.20 39.40 39.60 39.80 40.00 m/z 146.95 — 75.33% Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethy isilyl) e 147 73 5000 39.20 39.40 39.60 39.80 40.00 295 m/z 221.05 58.43% ........... .................. ............ 119 i —193 221........ .................... m/z-> . ... m 1 > 11 i n111 r. ।... fi...111111111111.a ।.... ।.... ।..111.11.।.... ।.... ।... 11. 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48514: N-Benzhydrylidene-1-(2,4,6-trimethylphenyl)ethylami 147 39.20 39.40 39.60 39.80 40.00 5000 m/z 281.00 27.24%
, ">65 , 197 312 343 n' |1' TTUTT 11111111 n 11" " । .. 11... ।. 11. H11... ।.... ।.. 111 < < 1. ।. 1.. p... ।.... |.... ।.... ।... 11. miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #70005:1,2-Bis(trimethylsiloxy)ethane 147 39.20 39.40 39.60 39.80 40.00 m/z 355.05 22.76% ............. / 73 5000
103 191
m/z-> 47 TVIIUITTTTT ++ <.।|>11।।।k..11 <>>>।>< t. ।। 40 60 80 100120140160180200220240260280300320340360380400420 ।«11 39.20 39.40 39.60 39.80 40.00
28263.D GCMS1126.M Fri Nov 30 13:41:35 2001 Page 6
NYC-WTC_000034193
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NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035700
Laboratory notes stating the GCMS scan of sample AD28901 revealed no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder