GCMS unknowns analysis results for sample AD28335, Jan 2002

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Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\JANO 802\28355A.D Vial: 4 Acq On 8 Jan 2002 6:13 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************** ************* Peak Number 18 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 35.42 7.89 ug/1 1625810 Perylene-dl2 36.91 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-l,z1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 42 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 N-Benzhydrylidene-1-(2,4,6-trimethy 343 C24H25NO 089839-57-6 27 4 1,2- Benzenedicarboxylic acid, bis (t 310 C14H2204Si2 002078-22-0 25 Abundance 73 Scan 3309 (35.419 min): 28355A.D (-) m/z J 100.00% 147 5000 221 281 355 429 35.00 35.20 35.40 35.60 35.80 45 117 TTTTTTTTT TT 1911—....................................... rn/z 147.0,0 51.79%

L. miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3 1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ........ — 147 35.00 35-20 35,40 35.60 35.80 m/z 221.05 32.12% 221 281 327 415 519I I I561 . L .. ,..,. T..,..T ..‘.. TTT PTrgur ( I ■ ' i > । ■ ^ । 1 1 1 ' I 1 1 1 1 I 1 ' 1 1 I 1 ' ' T *I miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71005: Ethanedicic acid, bis(trimethylsilyl) ester 73 -- e . — PPPP 147 35.00 35.20 35.40 35.60 35.80 5000- m/z 281.00 16.99% 45 117 , 190 219 1 1 • r 1 TT TTTT T 1. TTT — TPP -I.. ।.. TTT , TT m/z-_ Abundance 50 100 150 200 250 300 350 400 450 500 550 #48514: N-Benzhydrylidene-1-(2,4,6-trimethyiphenyi)ethylami ....I. .. p.y. ,. — . =.. pi I — 147

A 35.00 35.20 35.40 35.60 35.80 m/z 355.05 14.60% 5000

182 312< "i 343 ■ ' iT1 TTIP TTT । TIT TTTTeemTT IT CEETTT I 1 I I i i I 7 TTT.n. ■. T miz-> 50 100 150 200 250 300 350 400 450 500 550 35.00 35.20 35.40 35.60 35.80

28355A.D GCMS1126.M Wed Jan 09 09:10:21 2002 Page 18

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